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Abstrak :
ABSTRAK

Thermal spray sering diaplikasikan pada leading edge bilah turbin uap untuk meningkatkan ketahanan abrasi. Stellite adalah salah satu material yang sering digunakan dikarenakan ketahanannya yang baik terhadap aus. Penelitian ini bertujuan untuk mengkomparasi properti metode flame spray, plasma spray, dan HVOF dalam mendeposisikan lapisan Stellite ke bilah turbin baja tahan karat martensitik 410. Hasil lapisan plasma spray dan HVOF menunjukkan deposisi lapisan yang rata sedangkan flame spray tidak. Ketiga proses thermal spray memenuhi spesifikasi kuat lekat minimum manufaktur. Rata-rata kuat lekat dan kekerasan tertinggi didapat dari proses HVOF dengan nilai masing-masing 33,1 MPa dan 719 HV. Berdasarkan standar deviasi kuat lekat dan kekerasan, proses HVOF memiliki hasil lapisan paling homogen. Kekerasan substrat di bawah antarmuka pasca proses pelapisan flame spray, plasma spray, dan HVOF masing-masing naik sebesar 236%, 56%, dan 65% dari spesifikasi substrat. Lapisan HVOF memiliki tampilan penampang yang paling baik. Persentase porositas, diameter porositas, dan rata-rata panjang unbonding terkecil didapat pada proses HVOF dengan nilai masing-masing 0,2%, 7,2 μm, dan 31%. Struktur mikro lapisan pasca pengetsaan menghasilkan fasa-fasa yang berhubungan dengan masukan panas. Struktur dendritik terbentuk pada lapisan proses flame spray dan plasma spray pasca pengetsaan, namun tidak pada proses HVOF. Oksida dan karbida kobalt maupun krom mungkin terbentuk pada lapisan.

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ABSTRACT

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Thermal spray is often applied on steam turbine blade leading edge to increase abrasion resistance. Stellite is one of the commonly used material as it is known to wear protection against abrasion, oxidation, and corrosion at elevated temperature. Thermal spray method generally used in industry are flame spray, plasma spray, and HVOF. This research is intended to compare properties of those methods in depositing Stellite coating on 410 martensitic stainless steel turbine blade. Plasma spray and HVOF coating show even deposition while flame spray coating not. Those three coatings meet manufacture minimum bond strength requirement. On the flame spray process, higher preheat temperature resulted in higher bond strength. Preheat temperature variation relatively not affect coating hardness. Highest average bond strength and hardness are got by HVOF process with a value of 4.799 psi (33,1 MPa) and 719 HV respectively. According to bond strength and hardness standard deviation, the HVOF process gives the most homogeneous coating. Substrate hardness just below the coating interface after flame spray, plasma spray, and HVOF process are raised by 236%, 56%, and 65% each from the specification. HVOF coating has the best cross section compared to others with little splat and porosity. Flame spray coating has the most significant and highest amount of porosity.  In terms of percentage and size, HVOF gives the best result with a value of 0,2% and 7,2 μm respectively. The smallest coating interface unbonding is got by the HVOF process, with an average of 31%. Flame spray, plasma spray, and HVOF coating microstructure after etching show phases related to heat input during application. The dendritic structure is observed on flame spray and plasma spray coating after etching but not on HVOF process. Oxides like Cr₂O₃, CoCr₂O₄, CoO, and carbides like CoC, Cr₇C₃, Co₆W₆C, or Cr₂₃C₆ probably formed in the coating based on EDS result. Moreover, chemical composition result also indicates the formation of silicon oxide on coating and iron oxide at the coating interface. 

Abstrak :
Selama beberapa tahun terakhir, penggunaan teknik pelapisan permukaan oleh industri manufaktur telah mengalami peningkatan secara signifikan, terutama pada industri manufaktur katup (valve). Salah satu teknik pelapisan permukaan yang dipakai adalah pengerasan permukaan (hardfacing). Proses pengerjaan logam ini menggunakan bahan yang lebih keras untuk diterapkan pada permukaan logam dasar agar terjadi peningkatan ketahanan terhadap abrasi, korosi, dan benturan maupun jenis keausan lainnya, terutama yang berkaitan dengan pencegahan bagian-bagian mesin terhadap kekuatan destruktif pada kilang dan pabrik kimia, tenaga uap dan pembangkit nuklir. Penelitian ini bertujuan untuk meningkatkan ketahanan aus permukaan baja A216 WCB menggunakan pelapis berbahan Stellite 6. Pada penelitian ini parameter pelapisan permukaan menggunakan pelapis material Stellite 6 and penambahan pelapis antara (stainless steel ER309) sebelum pelapisan dengan stellite 6. Proses pelapisan permukaan baja karbon A216 WCB dilakukan dengan 2 layer kawat las stellite yang menggunakan proses pengelasan Tungsten Inert Gas (TI atau Gas Tungsten Arc Welding (GTAW). Sifat mekanis dan struktur mikro dilakukan pada produk pelapisan tersebut yaitu uji kekerasan, uji ketahanan aus dan pengamatan struktur mikro lapisan permukaan menggunakan mikroskop optic dan Scanning Electron Microscop (SEM) serta analisis presipitat serta fasa yang terbentuk diamati dan dievalusi menggunakan EDS. Hasil yang diperoleh dari penelitian yaitu struktur mikro hasil pengelasan pada bagian logam las stellite 6 menghasilkan struktur yang lebih mengarah ke kolumnar. Nilai kekerasan tertinggi dihasilkan oleh stellite double layer, yaitu sebesar 443 HV, nilai uji aus tertinggi juga didapatkan pada benda uji stellite  double layer, yaitu sebesar 0.281 x 10-6 mm3/mm. buttering 309 dipilih untuk menurunkan nilai kekerasan sehingga tidak rawan terjadinya retak pada benda uji.

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Over the past few years, the use of surface coating techniques by the manufacturing industry has increased significantly, especially in the valve manufacturing industry. One of the surface coating techniques used is surface hardening (hardfacing). This metalworking process uses harder materials to be applied to the surface of the base metal to increase resistance to abrasion, corrosion, and other types of wear and tear, especially those related to preventing machine parts from destructive forces at refineries and chemical plants, power steam and nuclear power plants. This study aims to improve the wear resistance of A216 WCB steel surfaces using Stellite 6 coating. In this study the surface coating parameters use Stellite 6 material coatings and the addition of intermediate coatings (stainless steel ER309) before coating with stellite 6. The process of coating A216 carbon steel surfaces performed with 2 layers of stellite welding wires using the Tungsten Inert Gas (TI) welding process Mechanical properties and microstructure are carried out on these coating products namely hardness test, wear resistance test and observation of microstructure of surface layers using a microscope optics and Scanning Electron Microscop (SEM) as well as precipitate analysis and formed phases are observed and evaluated using EDS The results obtained from the study are the microstructure of welding results on the stellite 6 weld metal section produces a structure that is more directed to the columnar.The highest hardness value in ih produced by double layer stellite, which is equal to 443 HV, the highest wear test value is also obtained on the double layer stellite test object, which is equal to 0.281 x 10-6 mm3/mm. 309 buttering was chosen to reduce the value of hardness so that it is not prone to cracking in the test specimens.