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"Komposit keramik yang berbasis Al2O3 adalah material yang potensial untuk aplikasi temperatur tinggi. Reaksi antarmuka yang terjadi diantara matriks dan penguat penting dan merupakan penentu atau peran kunci dalam kemajuan aplikasi dari komposit keramik. Proses directed metal oxidation (dimox) merupakan salah satu proses pembuatan komposit matriks keramik yang fleksibel dan menawarkan kemampuan untuk membentuk komposit near-net shape dengan bermacam-macam komposisi dan mikrostruktur. Keberhasilan pembuatan komposit Al2O3/Al dengan proses ini dipengaruhi oleh dopant, waktu tahan, temperatur dan atmosfir tempat berlangsungnya proses.Penelitian ini dilakukan dalam rangka menghasilkan komposit matriks keramik yang memiliki sifat mekanik yang baik dan antarmuka yang baik pula sebagai hasil dari reaksi antarmuka matriks dan penguat dalam meningkatkan ketangguhan dari matriks keramik. Temperatur proses yang digunakan 1100°C, 1200°C dan 1300°C dengan lamanya pemanasan 10 jam, 15 jam dan 24 jam untuk lingkungan atm dan temperatur proses yang digunakan untuk lingkungan N2 adalah 1100°C, 1150°C dan 1200°C dengan lamanya pemanasan 15 jam dengan persentase Mg sebagai dopant 5, 8, 10, 12 %. Hasil penelitian menunjukkan kedalaman infiltrasi maksimum dicapai pada waktu tahan proses 24 jam dengan 12% Mg dan temperatur 1300°C sebesar 29,34 mm, densitas maksimum dicapai pada waktu tahan proses 24 jam dengan 8% Mg pada temperatur 1100°C sebesar 3,50 gr/cm3, kekerasan mikro optimum dicapai pada waktu tahan proses 24 jam dengan 8% Mg dan temperatur 1100°C sebesar 1221 VHN, nilai fracture toughness maksimum pada waktu tahan proses 24 Jam dengan persentase 5% Mg dan temperatur 1300°C sebesar 8,25 MPa.m1/2. Reaksi antarmuka yang terbentuk dalam KMK Al2O3/Al adalah Al2O3, MgAl2O4, Mg3N2, AlN, AlSiO and MgSiO3.

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Al2O3 based ceramic composites are potential materials for advanced temperature applications. Interfacial reaction that °Ccurs between the matrix and the reinforcement is the critical, determinant and the key role in advancing the application of ceramic composites. Directed melt oxidation (dimox) pr°Cess is one of the flexible way to produce ceramic matrix composites that offer the ability to form near-net shape composites in various compositions and microstructures. The successful manufacturing of Al2O3/Al composite using dimox pr°Cess is influenced by the dopant, holding time, temperature and the atmospheric circumstances on the site of the pr°Cess.The research was performed in order to produce ceramic matrix composites that have reliable mechanical properties and good interface as a result of matrix interface and reinforcement reaction in improving the toughness of matrix ceramic. Pr°Cess temperature was set up at 1100 °C, 1200 °C and 1300 °C for 10 hours, 15 hours and 24 hours in furnace atmosphere, while the temperature pr°Cess was set up at 1100 °C, 1150 °C and 1200 °C in N2 atmosphere for 15 hours with the same Mg content various from 5, 8, 10 and 12% wt of Mg as the dopant. The results indicated that the maximum depth of infiltration was 29.34 mm achieved in 24 hours sample with 12% wt of Mg at 1300 °C. Generated density was 3.50 gr/cm3 which was the maximum density after 24 hours of the pr°Cess with 8% wt of Mg at 1100 °C. The optimum microhardness of 1221 VHN was achieved in 24 hours at 1100 °C with 8% wt of Mg. The maximum value of fracture toughness of 8.25 MPa.m1/2 which was achieved in 24 hours for sample with 5% wt of Mg at 1300 °C. The interfacial reaction was analyzed by XRD, content of phase that was formed by Al2O3/Al CMCs were Al2O3, MgAl2O4, Mg3N2, AlN, AlSiO and MgSiO3."

"Keramik merupakan material yang memiliki kekerasan yang sangat tinggi dan getas (getas). Untuk meningkatkan ketangguhan keramik,maka dikembangkan CMCs (Ceramic Matix Composite). Salah satu metode untuk memproduksi CMCs adalah dengan melalui proses DIMOX, yaitu cara mengoksida leburan logam dalam atmosfer dapur. Karakteristik produk CMCs yang dihasilkan melalui metode ini dipengaruhi oleh variabel waktu tahan, temperatur, dopant serta atmosfer tempat berlangsungnya proses pembentukan komposit.Penelitian ini bertujuan untuk mempelajari proses pembuatan CMCs C/Al melalui proses DIMOX dan pengaruh waktu tahan terhadap karakteristik produk CMCs yang dihasilkan. Pada penelitian ini dilakukan variasi waktu tahan, dimana digunakan waktu tahan 8, 10, 15, 20, 24 jam pada temperatur 1100 °C. Karakterisasi terhadap produk komposit yang dihasilkan dilakukan melalui pengujian densitas dan porositas, pengujian kekerasan mikro, pengamatan struktur mikro dengan menggunakan mikroskop optik dan SEM serta pegujian komposisi kimia.Infiltrasi prabentuk C oleh leburan Al dapat terjadi secara optimum pada waktu tahan 24 jam. Produk CMCs dengan densitas yang tertinggi, sebesar 3,17 gram/cm3, diperoleh pada waktu tahan 24 jam. Porositas produk CMCs cenderung meningkat seiring dengan penambahan waktu tahan. Produk CMCs dengan kekerasan mikro tertinggi, sebesar 14300 Mpa pada waktu tahan 24 jam. Laju keausan produk CMCs tertinggi, sebesar 2.03x10^-6 m3/mm terdapat pada waktu tahan 24 jam. Partikel C terdistribusi cukup merata pada produk CMC C/Al. Pada produk CMCs pada daerah sekitar partikel C dapat ditemui adanya Al, spinel (MgAl2O4), Al2O3.

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Ceramic is material which possed a very high hardness and brittle. To increase its toughness, then CMCs is developed. One of method to produce CMCs is DIMOX process. DIMOX involved oxidized molten metal in furnace atmosphere. The charateristic of CMCs product is effected by variables processes such as : holding time, temperature, dopant and the atmosphere where the process is held.

The aim of this research is to study the making process of CMCs C/Al itself through DIMOX process and the effect of holding time with variable : 8, 10, 15, 20, 24 hours at 1100 °C. The characterizations of CMCs are examined by density, porosity, hardness, wear and microstructure analysis.

It is found that Infiltration preform graphite by molten Al is optimal at the holding time of 24 hours. This variable produced highest density at 3,17 gr/cm3. The porosity of CMCs product tends to increase with increment of holding time. The highest porosity that obtained at holding time of 24 hours is 6.15 %. The highest hardness that can be obtained at holding time of 24 hours is 14300 MPa. This variable also produced the lowest wear rate, it is 2.03x10^-6 mm3/mm. Distribution of graphite particles spread over C / Al composite product and around graphite particles can be found Al, spinel ( MgAl2O4 ), and Al2O3. Based on EDS analysis, there are three phase in systems of CMCs product, they are C/Al, Al2O3/Al, and C/Al2O3."

"This research is to study the effects of _firing temperature and holding time on characteristics of Directed Metal Oxidation (DIMOAQ Ceramic Matrix Composites (CMCs) SiC /' A1 product. In this research, the firing temperature and holding time used are varied from 900° C to 1300° C with holding time 10 and 20 hours for each temperature. The characterizations of composite products are examined such as density and porosity test, micro hardness test, microstructure examination and chemical composition test. The results show that SiC preform has been infiltrated by Al liquid at tiring temperature of 1100"C for 20 hours. Composite product with the highest density (3,54 gram / cm3) can be obtained at firing temperature of 1100°C for 20 hours. Porosity tents to increase with increasing firing temperature. Composite product with highest micro hardness (1820 VHM can be obtained at firing temperature of 1300°C for 10 hours. At the some firing temperature, composite at products micro hardness for 20 hours tower than composite product with holding time I0 hours. Distribution of SiC particles spread over quite uniform on SiC/A1 composites product. Around SiC particles can be found Al, spinel (MgAl2O2). Al2O2, and possibility Mg,Si."