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Abstrak :
ABSTRAK
Material stainless steel 304 SS 304 merupakan logam paduan dari beberapa unsur utama yakni Fe, Cr dan Ni yang memiliki karakteristik yang baik yakni tahan terhadap korosi sehingga aplikasinya banyak digunakan dalam berbagai bidang termasuk pada sektor minyak dan gas. Disamping memiliki keunggulan yang tahan terhadap korosi, SS 304 memiliki kelemahan untuk penggunaan pipa minyak yakni sifat kekerasan yang cukup rendah bila dibandingkan dengan stainless steel jenis lainnya. Karena kelemahan tersebut mengakibatkan SS 304 tidak cocok untuk aplikasi yang membutuhkan kinerja tinggi pada sifat mekanik. Dalam penelitian ini telah dilakukan rekayasa sifat mekanik permukaan material SS 304melalui tiga perlakuan yakni cold rolling dengan tingkat reduksi 0 hingga 80 , annealing pada temperatur 400 0C, 600 0C, 800 0C dan 1000 0C dengan waktu tahan selama 1 jam dan proses boronisasi menggunakan boraks sebagai sumber boron. Proses boronisasi dilakukan pada temperatur bervariasi dimulai pada temperatur 750 0C, 850 0C, 950 0C dan 1050 0C dengan waktu penahanan selama 4 jam, 6 jam, 8 jam dan 8 jam quenching.Diperoleh hasil bahwa efek pengerjaan dingin melalui cold rolled dengan tingkat deformasi 20, 40, 60 dan 80 adalah disamping terjadi transformasi fasa dari austenite menjadi martensite juga perubahan morfologi struktur fasa material dari awalnya dengan morfologi kristal equiaxial menjadi elongated crystal pipih panjang dengan tingkat orientasi kristal yang semakin tinggi dengan meningkatnya tingkat deformasi. Perubahan mikrostruktur karena deformasi oleh cold rolled berhasil meningkatkan nilai kekerasan berturut-turut dimulai dari 145 HV pada sampel uji bebas deformasi, 349 HV, 388 HV, 410 HV dan menjadi 450 HV pada sampel uji dengan tingkat deformasi 80 . Demikan juga dengan ketahanan aus sampel uji mengalami peningkatan dari 10,11 mm3/mm pada sampel bebas deformasi menjadi 5,88 mm3/mm pada sampel uji deformasi 80 .Studi mikrostruktur pasca perlakuan anil pada sampel uji terdeformasi 40 dan 80 memperlihatkan terjadinya transformasi fasa dari martensit menjadi austenit pada kedua jenis sampel uji. Perlakuan anil pada berbagai temperatur cenderung mengembalikan mikrostruktur awal yaitu kembali terdiri dari fasa dominan austenit. Secara umum diketahui bahwa kedua sampel uji memiliki nilai kekerasan terendah dibandingkan dengan nilai kekerasan sampel uji pasca anil pada temperatur anil yang lebih rendah. Nilai kekerasan dan ketahanan aus kedua sampel uji memperlihatkan nilai yang hampir sama masing-masing sebesar 146 HVC dan 8,51 mm3/mm pada sampel terdeformasi 40 dan 153 HVC dan 8,66 mm3/mm pada sampel uji terdeformasi 80 pasca perlakuan anil pada temperatur 1000 0C. Sedangkan efek boronisasi mengggunakan borax sebagai sumber boron melalui permukaan menghasilkan lapisan difusi terdiri dari fasa Fe2B dan fasa Fe2O3 sebagai fasa tambahan disamping fasa awal berupa fasa austenit dan martensite. Boronisasi pada temperatur 950 0C dengan waktu tahan 8 jam mampu meningkatkan kekerasan permukaan sampel uji mencapai 588 HV jauh melebihi nilai yang dicapai melalui efek deformasi. Kecenderungan yang sama terhadap sifat mekanik ketahanan aus yaitu terjadi peningkatan dari 10,6 mm3/mm menjadi 7,3 mm3/mm. Penelitian ini menyimpulkan bahwa efek perlakuan melalui proses boronisasi pada temperatur 950 0C efektif untuk meningkatkan kekerasan dan ketahanan aus sampel SS 304.

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ABSTRACT
The 304 stainless steel SS 304 is an alloy consisted of main elements Fe, Cr and Ni which exhibit good corrosion resistant characteristics. The SS304 has met wide applications in various fields including oil and gas sectors. Although the SS304 has a good corrosion-resistant, it has however a weakness in some mechanical properties which are quite low when compared with other types of stainless steels. Because of such weaknesses, SS304 is not suitable for applications that require high performance on mechanical properties. In the current research works, improvement in the mechanical properties of SS304 especially the hardness and wear resistance were carried out through cold rolled deformation and heat treatment. An additional surface treatment, allowing the diffusion process through boronization of two different boron source was also studied. The cold rolled treatment resulted in deformed samples with 0 to 80 thickness reduction. The heat treatment studies to the samples were carried out under annealing at the following temperatures: 400 0C, 600 0C, 800 0C and 1000 0C for 1 hour holding time. The process of boronization was carried out at 750 0C, 850 0C, 950 0C and 1050 0C with holding times of 4 hours, 6 hours, 8 hours and 8 hours followed by quenching for each temperature.It is shown that the phase transformation from austenite to martensite has taken place in all deformed samples in which fully martensite was obtained in a deformed sample of 80 thickness reduction. In addition, the morphological changes of the phase structure from the equiaxial grain morphology to the elongated flat-length grains with a prefer orientation to the rolling direction occurred in all deformed samples. It was found that the higher deformation rate experienced by the samples, the greater the orientation level. The crystal orientation is getting higher with increasing levels of deformation. The microstructural changes due to deformation by cold rolled succeeded in increasing the hardness value of 145 HV in the deformation free test sample, 349 HV, 388 HV, 410 HV to 450 HV on the test sample with a 80 deformation rate. Similarly with the wear resistance of the test sample having an increase of 10.11 mm3/mm in the deformation-free sample being 5.88 mm3/mm in the 80 deformed sample.The microstructural studies due to the annealing effect on the post-deformation test sample of 40 and 80 showed the occurrence of phase transformation from martensite to austenite in both types of test samples. Annealing treatment to the deformed samples at various temperatures tends to restore the initial microstructure which dominated by austenite. It is generally known that the two test samples have the lowest hardness value compared to the value of the hardness of the post-annealed sample at lower annealing temperatures. The hardness and wear resistance values of both samples exhibited almost the same values ?? ??of 146 HVC and 8.51 mm3/mm respectively in the 40 deformed sample and 153 HVC and 8.66 mm3/mm in the 80 deformed sample after annealing treatment at a temperature of 1000 0C. While boronization effect using borax as a source of boron through the surface produce diffusion layer consists of Fe2B and Fe2O3 phases as the additional phases to the initial phases of austenite and martensite. Boronization at a temperature of 950 C has increased the surface hardness reach 588 HV which is far above the value achieved through the deformation effect. The same tendency was also applied to the wear resistance in which an increase from 10.6 mm3/mm to 7.3 mm3/mm. This study concluded that the treatment effect through the boronization process at 950 C is more effective for increasing hardness and wear resistance of SS 304 samples.

Abstrak :
Penelitian ini bertujuan untuk mengetahui pengaruh pelapisan nikel dengan metode impregnasi basah pada substrat katalitik stainless steel 316 terhadap yield dan kualitas carbon nanotube CNT berbasis limbah polipropilena PP menggunakan reaktor flame synthesis. Dilakukan variasi loading nikel sebesar 0 , 5 dan 10 . Hasil penelitian menunjukkan pelapisan nikel dapat meningkatkan yield CNT namun tidak signifikan, yaitu hanya sebesar 8,4. Akan tetapi, hasil CNT yang dihasilkan dari pelapisan nikel dengan loading 10 pada substrat SS 316 memiliki kualitas yang lebih baik. Dari hasil XRD, CNT terdeteksi pada peak intensitas 2 = 26° dan 43°, serta masih terdeteksi beberapa pengotor berupa grafit, Fe3O4, Fe3C, dan NiO pada ketiga sampel. Hasil SEM menunjukkan CNT lebih banyak terbentuk pada substrat dengan loading nikel 10 , dan ketiga sampel masih terdapat karbon amorf dan pengotor lain. Hasil EDX menunjukkan persen berat karbon dari sampel CNT yang tumbuh pada substrat loading nikel 10 lebih tinggi dari sampel lain, yaitu 74,07. Pada hasil TGA, pelapisan nikel dapat meningkatkan stabilitas termal CNT karena CNT mengalami penurunan persen massa pada suhu oksidasi sebesar 620oC. Karena peningkatan yield yang tidak signifikan pada limbah PP, dilakukan uji pelapisan nikel pada substrat stainless steel dengan sumber karbon kamper. Yield yang dihasilkan juga tidak signifikan, hanya sebesar 6,8. Namun, kualitas CNT yang dihasilkan justru mengalami peningkatan, baik dari segi diameter kristal yang menjadi semakin kecil sebesar 8,08 nm, komposisi karbon yang meningkat sebesar 83,06, maupun stabilitas termal yang meningkat dengan suhu oksidasi sebesar 723°C. Oleh karena itu, pelapisan nikel dapat meningkatkan yield meskipun tidak signifikan serta dapat meningkatkan kualitas CNT.

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This research aims to determine the effect of nickel coating on 316 stainless steel catalytic substrate by wet impregnation method on the yield and quality of polypropylene waste based carbon nanotube CNT using a flame synthesis reactor. The effect of nickel loading was studied at 0 , 5 and 10 . The results showed nickel coating increase CNT yield by 8.4 . However, CNT with 10 nickel loading offered the best yield and quality.. From the XRD results, CNT was detected at peak intensities of 2 26° and 43°, and still detected some impurities such as amorphous carbon, Fe3O4, Fe3C and NiO. From the SEM results showed that more CNT were produced on substrate with 10 nickel loading. EDX result shows that the carbon weight percentage from CNT with 10 nickel loading substrate is higher than other samples, which is 74.10 . In the TGA results, nickel coating can increase the thermal stability of CNT because CNT mass has decreased at an oxidation temperature of 620oC. Because the CNT yield from PP waste is not significant, nickel coating on substrates is tested with camphor as carbon sources. The yield produced is also insignificant by 6.8 . However, the quality of CNT is increased, in terms of crystal diameter which became smaller by 8.08 nm, the composition of carbon which increased by 83.06 , and the thermal stability which increased with an oxidation temperature of 723°C. Therefore, nickel coating can increase yield even it is not significant and can improve the quality of CNT.

Abstrak :
[Stainless steel merupakan material yang paling banyak digunakan dalam pembuatan turbin pembangkit tenaga listrik Organic Rankine Cycle (ORC), karena densitasnya yang tinggi, membuat kinerja turbin menjadi kurang efisien. Salah satu alternatif penggantinya adalah paduan aluminium seri 7xx.x (Al-Zn-Mg) yang memiliki sifat mekanik terbaik dibandingkan dengan seri yang lainnya. Sifat mekanik paduan tersebut dapat ditingkatkan dengan penambahan Cr serta perlakuan pengerasan penuaan. Pada penelitian ini dipelajari pengaruh penambahan Cr sebesar 0, 0.03, 0.1 dan 0.46 wt. % pada paduan Al-10Zn-6Mg. Paduan dibuat dengan proses squeeze casting dengan tekanan sebesar 76 MPa. Pelat selanjutnya dihomogenisasi pada temperatur 400 oC selama 4 jam dan dilakukan proses pengerasan penuaan dengan melakukan solution treatment pada temperatur 440 oC selama 2 jam, pendinginan cepat, dan penuaan pada temperatur 130 oC. Karakterisasi yang dilakukan diantaranya adalah pengujian kekerasan Rockwell B, pengujian impak, pengamatan struktur mikro dengan mikroskop optik dan Scanning Electron Microscope (SEM) dilengkapi dengan Energy Dispersive X-Rays (EDX), dan Simultaneous Thermal Analysis (STA). Hasil penelitian menunjukkan bahwa penambahan Cr sebesar 0.03, 0.1 dan 0.46 wt. % meningkatkan kekerasan paduan Al-10Zn-6Mg menjadi 50.9, 52.8, 53.2 HRB yang diakibatkan oleh pengecilan ukuran SDAS, pembentukan larutan padar Cr di dalam matriks serta pembentukan fasa kedua (CrFe)Al7 dan CrAl7 pada penambahan 0.46 wt. % Cr. Penambahan Cr belum memberikan pengaruh yang signifikan terhadap proses pemanasan. ......Stainless steel is most widely used in manufacturing of turbine impeller of Organic Rankine Cycle (ORC). However, due to its high density, the performance of turbine becomes less efficient. One alternative to substitute stainless steel is 7xx.x series aluminum alloys (Al-Zn-Mg) which have good mechanical properties compared to other series. Their mechanical properties can be improved by the addition of Cr as well as precipitation hardening process. This research studied the effect of addition of Cr with variation of 0, 0.03, 0.1 and 0.46 wt. % in Al-10Zn-6Mg alloys. The samples were made by squeeze casting process with pressure of 76 MPa. The plate was then homogenized at 400 ° C for 4 hours, followed by precipitation hardening process which consisted of solution treatment at 440 ° C for 2 hours, water quenching and ageing 130 ° C. Characterization was done by Rockwell B hardness testing, impact testing, microstructure observation by using optical microscope and Scanning Electron Microscope (SEM) equipped with Energy Dispersive X-rays (EDX) and Simultaneous Thermal Analysis (STA). The results showed that addition of Cr 0.03, 0.1 and 0.46 wt. % increase the hardness of Al-10Zn-6Mg aloys to 50.9, 52.8, 53.2 HRB respectively, which were due to reduction of SDAS, solid solution strengthening of Cr in the matrix and the formation of (CrFe)Al7 and CrAl7 second phases when 0.46 wt. % Cr was added. During ageing process also increased hardness alloys, but Cr were not have a significant impact on the transformation phase. The addition of Cr not have a significant influence on the heating process. ;Stainless steel is most widely used in manufacturing of turbine impeller of Organic Rankine Cycle (ORC). However, due to its high density, the performance of turbine becomes less efficient. One alternative to substitute stainless steel is 7xx.x series aluminum alloys (Al-Zn-Mg) which have good mechanical properties compared to other series. Their mechanical properties can be improved by the addition of Cr as well as precipitation hardening process. This research studied the effect of addition of Cr with variation of 0, 0.03, 0.1 and 0.46 wt. % in Al-10Zn-6Mg alloys. The samples were made by squeeze casting process with pressure of 76 MPa. The plate was then homogenized at 400 ° C for 4 hours, followed by precipitation hardening process which consisted of solution treatment at 440 ° C for 2 hours, water quenching and ageing 130 ° C. Characterization was done by Rockwell B hardness testing, impact testing, microstructure observation by using optical microscope and Scanning Electron Microscope (SEM) equipped with Energy Dispersive X-rays (EDX) and Simultaneous Thermal Analysis (STA). The results showed that addition of Cr 0.03, 0.1 and 0.46 wt. % increase the hardness of Al-10Zn-6Mg aloys to 50.9, 52.8, 53.2 HRB respectively, which were due to reduction of SDAS, solid solution strengthening of Cr in the matrix and the formation of (CrFe)Al7 and CrAl7 second phases when 0.46 wt. % Cr was added. During ageing process also increased hardness alloys, but Cr were not have a significant impact on the transformation phase. The addition of Cr not have a significant influence on the heating process. , Stainless steel is most widely used in manufacturing of turbine impeller of Organic Rankine Cycle (ORC). However, due to its high density, the performance of turbine becomes less efficient. One alternative to substitute stainless steel is 7xx.x series aluminum alloys (Al-Zn-Mg) which have good mechanical properties compared to other series. Their mechanical properties can be improved by the addition of Cr as well as precipitation hardening process. This research studied the effect of addition of Cr with variation of 0, 0.03, 0.1 and 0.46 wt. % in Al-10Zn-6Mg alloys. The samples were made by squeeze casting process with pressure of 76 MPa. The plate was then homogenized at 400 ° C for 4 hours, followed by precipitation hardening process which consisted of solution treatment at 440 ° C for 2 hours, water quenching and ageing 130 ° C. Characterization was done by Rockwell B hardness testing, impact testing, microstructure observation by using optical microscope and Scanning Electron Microscope (SEM) equipped with Energy Dispersive X-rays (EDX) and Simultaneous Thermal Analysis (STA). The results showed that addition of Cr 0.03, 0.1 and 0.46 wt. % increase the hardness of Al-10Zn-6Mg aloys to 50.9, 52.8, 53.2 HRB respectively, which were due to reduction of SDAS, solid solution strengthening of Cr in the matrix and the formation of (CrFe)Al7 and CrAl7 second phases when 0.46 wt. % Cr was added. During ageing process also increased hardness alloys, but Cr were not have a significant impact on the transformation phase. The addition of Cr not have a significant influence on the heating process. ]

Abstrak :
ABSTRAK
Metal Injection Moulding MIM merupakan suatu metode aplikasi dari Metalurgi Serbuk PM dan Plastic Injection Moulding yang sedang banyak dikembangkan untuk pembuatan komponen-komponen kecil yang presisi. Teknologi ini dikenal dengan kelebihan-kelebihannya seperti produktivitas tinggi, near-net-shape, permukaan akhir benda yang baik, dan kemampuan produk untuk diberikan perlakuan panas guna mencapai sifat yang diinginkan. Logam yang paling banyak diaplikasikan pada PM adalah stainless steel hasil fabrikasi dengan metode atomisasi gas yang menghasilkan serbuk dengan ukuran dan distribusi ukuran kecil, bentuk spherical, dan tingkat kemurnian serbuk yang tinggi dengan kandungan oksigen rendah

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ABSTRACT
Metal Injection Molding MIM is an application of Powder Metallurgy PM and Plastic Injection Moulding which is currently being developed to produce small yet precise components. This technology is known for its advantages such as high productivity, near net shape, good surface finish, and great heat treatability to achieve desirable properties. Most applied metal using PM is stainless steel fabricated by gas atomization that produces powder with small size and size distribution, spherical shape, and high purity powder with low oxygen content

Abstrak :
Aplikasi pengelasan dengan material yang berbeda mendapatkan keuntungan dari segi ekonomis. Pada penelitian ini digunakan material antara baja tahan karat austenitik dan baja karbon rendah SS 400 dengan jenis kawat las yang berbeda yaitu ER 309 dan ER 316 dengan metode GMAW. Hal ini bertujuan untuk melihat pengaruh dari sifat mekanis material. Untuk mengidentifikasi fase penyusun pada sambungan las tak sejenis dilakukan melalui mikroskop optik (OM), dan untuk menguji kekerasan dilakukan menggunakan micro Vickers untuk mendapatkan sifat mekanik lasan yang terdiri dari logam dasar (BM), daerah terpengaruh panas (HAZ), dan logam las (WM). Dari hasil percobaan didapatkan bahwa nilai kekerasan tertinggi ada pada daerah WM dan HAZ sebab memiliki butir yang lebih halus dibandingkan dengan logam induk. Butir yang halus ini akan membuat semakin banyak batas butir sehingga memiliki kekerasan yang lebih tinggi. Struktur mikro yang didapat pada BM dan HAZ SS 316 memiliki fasa austenit sedangkan BM dan HAZ SS 400 memiliki fasa ferit dan perlit. Pada daerah logam las (WM) dengan kawat las ER 309 memiliki kekerasan tertinggi sebesar 258 Hv dibandingkan dengan nilai kekerasan logam las menggunakan kawat las ER 316, 253 Hv, hal ini disebabkan karena adanya kandungan Cr yang lebih tinggi pada ER 309 (23,5%), dibandingkan dengan menggunakan kawat las ER 316 (19,25%). ......Welding applications with different materials have an economic advantage. In this study, materials between austenitic stainless steel and SS 400 low carbon steel were used with different types of welding wire, namely ER 309 and ER 316 with the GTAW method. It aims to see the effect on the mechanical properties of the welded joints. To identify the constituent phases of dissimilar welded joints, an optical microscope (OM) was carried out, and the hardness testing, micro Vickers was used to obtaining the mechanical properties of the weldment, which consists of base metal (BM), heat affected zone (HAZ), and weld metal (WM). The experimental results show that the highest hardness values are in the WM and HAZ regions because they have finer grains than the parent metal. These fine grains will create more grain boundaries so that they have higher hardness. The microstructure obtained in BM and HAZ SS 316 has an austenite phase, while BM and HAZ SS 400 have ferrite and pearlite phases. In the weld metal (WM) area with ER 309, the highest hardness is 258 Hv compared to the hardness value of welding metal using ER 316, 253 Hv. This is due to the higher Cr content in ER 309 (23.5 %) than ER 316 (19.25%).

Abstrak :
Progress in the understanding of corrosion and corrosion resistance properties of sintered stainless steels has lead to new applications that benefit from net shape processing and more efficient material utilization.