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"This book covers novel research results for process and techniques of materials characterization for a wide range of materials. The authors provide a comprehensive overview of the aspects of structural and chemical characterization of these materials. Includes a compilation of the best research works presented in Symposium 5B "Structural and Chemical Characterization of Metals, Alloys and Compounds," by XXIII International Materials Research Congress (IMRC-2014)."

"This volume contains the Proceedings of the RILEM TC 252-CMB International Symposium on the Chemo-Mechanical Characterization of Bituminous Materials.The Symposium was attended by researchers and practitioners from different fields presenting the latest findings in the chemical, mechanical, and microstructural characterization of bituminous materials. The book offers new and cutting edge papers on innovative techniques for the characterization of bituminous materials, gaining new insights into current issues such as effects of aging, moisture, and temperature."

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Teknik Neutron Scattering merupakan salah satu teknik yang berperan sangat penting terhadap perkembangannya teknologi baterai lithium-ion, yang dimana teknik ini digunakan untuk menginvestigasi kemampuan penyimpanan energi pada baterai lithium-ion. Pada prinsipnya neutron scattering memanfaatkan neutron yang mampu mendeteksi unsur-unsur yang sangat ringan dan menjadikan suatu kelebihan yang sangat penting pada teknik.neutron scattering. Mengingat pentingnya material penyimpanan energi seperti lithium-ion yang digunakan pada perangkat elektronik sehari-hari maka semakin besar tuntutan untuk membuat dan menemukan material baterai litihum-ion semakin berkembang pada life time, kemampuan cyclic dan stabilitasnya. Penelitian ini dilakukan untuk mempelajari cara penggunaan dan pemanfaatan teknik neutron beam scattering dalam mengidentifikasi struktur crystal dari sampel yang digunakan yaitu anoda ZnO, dengan menggunakan high resollution power diffraction (HPRD) di Badan Tenaga Nuklir Nasional (BATAN). Hasil yang didapat pada posisi 2 theta pada titik 114,32 derajat didapat grid parameter 2,899 yang dimana apabila dibulatkan sangat mendekati grid parameter unsur besi (Fe) yang bernilai 2,866 Angstorm. Namun belum terlihat unsur lain selain besi dikarenakan besarnya intensitas casing besi dari sample coin cell baterai.

 

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Neutron Scattering technique is one technique that plays a very important role in the development of lithium-ion battery technology, which is used to investigate the energy storage capabilities of lithium-ion batteries. In principle, neutron scattering utilizes neutrons which are capable of detecting very light elements and making a very important advantage in techniques. Neutron scattering. Considering the importance of energy storage materials such as lithium-ion used in everyday electronic devices, the greater the demand to make and find battery-litihum-ion materials increasingly develops on life time, cyclic ability and stability. This research was conducted to study how to use and use the neutron scattering technique in identifying the crystal structure of the sample used, namely ZnO anode, using high resistance power diffraction (HPRD) at BadaN National Nuclear Power (BATAN).

 

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"Pada penelitian ini medan magnet akan ditingkatkan untuk mendapatkan konstanta verdet yang bervariasi Kumparan dengan diameter 2 mm dan hambatan 1,5 Ohm dirancang untuk menghasilkan medan magnet kuat hingga mencapai 500 mT. Kumparan akan dilewatkan arus maksimum 20 A dan tegangan maksimum 30 V. Namun kumparan 2 mm yang dilewati arus sebesar 20 A akan menimbulkan panas berlebih yang mengganggu kestabilan besar medan magnet yang dihasilkan sehingga diperlukan penambahan sebuah sistem pendingin menggunakan blok air yang ditempelkan pada inti magnet dan kumparan. Apabila medan magnet kuat memengaruhi material mengneto-optik (MOE) fase cair yang dilewatkan cahaya maka disebut sebagai metode rotasi faraday. Metode rotasi faraday digunakan untuk mencari besar konstanta verdet. Konstanta verdet merupakan representasi karakteristik material magneto-optik (MOE) fase cair. Pada penelitian ini untuk mendapatkan nilai konstanta verdet, nilai yang diukur adalah besar medan magnet, besar sudut cahaya yang terpolarisasi, dan intensitas cahaya. Menggunakan cahaya laser merah berbentuk titik dengan panjang gelombang 650 nm dengan intensitas cahaya maksimum sebesar 54612 lux. Perubahan sudut dilakukan menggunakan gir yang terhubung degan stteper motor dan sistem analisator. Pengambilan data menggunakan teknik polarisasi yang terpengaruh oleh medan magnet eksternal. Nilai medan magnet yang terukur oleh teslameter dengan variasi antara -250—250 mT. Sudut rotasi faraday diperoleh dari selisih besar sudut polarisator dan analisator dengan selisih sudut mula-mula sebesar 45°. Cahaya yang melewati polarisator dan analisator akan terdeteksi oleh sensor cahaya BH1750. Hasil penelitian ini akan menunjukkan besar konstanta verdet dari setiap material magneto-optik (MOE) fase cair.

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In this research, the magnetic field will be increased to obtain a variable verdet constant. The coil with a diameter of 2 mm and a resistance of 1.5 Ohm is designed to produce a strong magnetic field up to 500 mT. The coil will pass a maximum current of 20 A and a maximum voltage of 30 V. However, a 2 mm coil that is passed by a current of 20 A will cause excessive heat which disrupts the stability of the large magnetic field produced, so it is necessary to add a cooling system using a water block attached to the magnetic core and coil. If a strong magnetic field affects the magneto-optic element (MOE) that is passed by light, it is called the Faraday rotation method. Faraday rotation method is used to find the verdet constant. The verdet constant is a representation of the characteristics of the liquid phase magneto-optic element (MOE). In this research to obtain the value of the verdet constant, the measured values are the magnitude of the magnetic field, the angle of polarized light, and the intensity of light. Using red laser light in the form of a point with a wavelength of 650 nm with a maximum light intensity of 54612 lux. Angle changes are carried out using gears connected to the stepper motor and analyzer system. Data retrieval using a polarization technique that is affected by an external magnetic field. The value of the magnetic field measured by the teslameter varies between -250—250 mT. Faraday rotation angle is obtained from the large difference between the polarizer and the analyzer angle with the initial angle difference of 45°. Light that passes through the polarizer and analyzer will be detected by the BH1750 light sensor. The results of this study will show the magnitude of the verdet constant of each liquid phase magneto-optic element (MOE)."

"Kebutuhan akan material penyerap gelombang elektromagnetik semakin tumbuh pada aplikasi militer dan juga pada aplikasi sipil. Material penyerap gelombang elektromagnetik yang selanjutnya akan disebut dengan Radar Absorbing Material (RAM), pada frekuensi tertentu akan melemahkan radiasi gelombang elektromagnetik yang datang dan mendisipasi energi yang diserap dalam bentuk panas. RAM berhasil dibuat dengan metode hand lay up yang tersusun dari carbon black/epoksi/E-Glass fiber. Variasi carbon black sebagai filler diberikan sebesar 0 wt%, 1 wt %, 3 wt %, dan 5 wt%. Karakterisasi penyerapan gelombang elektromagnetik RAM dilakukan dengan uji Vector Network Analyzer (VNA) pada pita frekuensi X-Band 8,2-12,4 GHz. Spesimen RAM dengan kandungan carbon black 5 wt% menunjukkan nilai reflection loss paling optimal sebesar -10,7 dB pada frekuensi 9,5 GHz dengan penyerapan gelombang EM mencapai 91,48 %.

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The need for an electromagnetic wave absorbing material has beengrowing formilitary as well as for civil application. Electromagnetic wave absorbing material which would be referred to the Radar Absorbing Material (RAM), at a certain frequency weakens the incoming electromagnetic wave radiation and dissipates the absorbed energy in the form of heat. RAM was successfully made by hand lay-up method which wascomposed of carbon black / epoxy / E-Glass fiber. Variation of carbon black as filler was given by 0 wt%, 1 wt%, 3 wt%, and 5 wt%. Characterization of the electromagnetic wave absorption ofRAM was conducted by Vector Network Analyzer(VNA) test on the X-Band frequency of 8.2 to 12.4 GHz. RAM with the 5 wt%carbon black showedthe most optimal value reflection loss of - 10.7 dB at 9.5 GHz with electromagentic wave absorption reached up to 91.48%."

"One of the key challenges current biomaterials researchers face is identifying which of the dizzying number of highly specialized characterization tools can be gainfully applied to different materials and biomedical devices. Since this diverse marketplace of tools and techniques can be used for numerous applications, choosing the proper characterization tool is highly important, saving both time and resources.Characterization of biomaterials is a detailed and multidisciplinary discussion of the physical, chemical, mechanical, surface, in vitro and in vivo characterization tools and techniques of increasing importance to fundamental biomaterials research.Characterization of biomaterials will serve as a comprehensive resource for biomaterials researchers requiring detailed information on physical, chemical, mechanical, surface, and in vitro or in vivo characterization. The book is designed for materials scientists, bioengineers, biologists, clinicians and biomedical device researchers seeking input on planning on how to test their novel materials, structures or biomedical devices to a specific application. Chapters are developed considering the need for industrial researchers as well as academics."

"Biomaterials and medical devices must be rigorously tested in the laboratory before they can be implanted. Testing requires the right analytical techniques. Characterization of biomaterials reviews the latest methods for analyzing the structure, properties and behaviour of biomaterials.Beginning with an introduction to microscopy techniques for analyzing the phase nature and morphology of biomaterials, Characterization of biomaterials goes on to discuss scattering techniques for structural analysis, quantitative assays for measuring cell adhesion, motility and differentiation, and the evaluation of cell infiltration and tissue formation using bioreactors. Further topics considered include studying molecular-scale protein-surface interactions in biomaterials, analysis of the cellular genome and abnormalities, and the use of microarrays to measure cellular changes induced by biomaterials. Finally, the book concludes by outlining standards and methods for assessing the safety and biocompatibility of biomaterials."